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美国麦克仪器公司作为材料表征行业的领导者,一直致力于为广大的研发人员提供精确、可靠的精密仪器,以引领行业发展为己任,全力支持中国材料科学的壮大发展。由麦克仪器公司全资支持的、将在下月首次颁发的麦克仪器-中国颗粒学会最佳论文奖为麦克仪器支持中国科学发展的又一力作。也基于此,广大研发人员选择麦克仪器,使用麦克仪器,不断地首选与引进麦克仪器的先进技术为其科学研究助力,使美国麦克仪器公司ASAP 2020全自动比表面与孔隙度分析仪成为行业内被论文引用最多的仪器。我们将继续努力,携手中国材料科学研究者为科学技术发展做出更多的贡献。
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文章摘要:
A major challenge in the implementation of laboratory-designed catalysts is the scale-up into technically relevant forms. Advanced characterization is essential to understand and optimize catalyst assembly and function in industrial reactors. This Article presents an integrated approach to visualizing millimetre-sized extrudates and granules of a hierarchical MFItype zeolite, displaying trimodal networks of micropores (0.56 nm), intracrystalline mesopores (∼10 nm) and macropores(∼200–300 nm). As exemplified for the conversion of methanol to olefins, the hierarchical zeolite yields a superior performance compared to its conventional analogue. The combination of dedicated specimen preparation with state-of-theart optical, X-ray and electron-based microscopic and tomographic techniques proves a powerful methodology to reveal otherwise inaccessible information regarding structural organization over the whole range of length scales. It is expected that these tools will play a crucial role in the rationalization of scale-up principles in catalyst development.